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Construction Of An Open Steam Distillation Column

6 Chapters
|
37 Pages
|
4,030 Words
|
Chemistry Education

Complete Construction Of An Open Steam Distillation Column Project Materials (Chapters 1 to 5):

ABSTRACT

We constructed an open steam distillation column with the following specifications:-
FOR THE COLUMN
Height of column = 500mm
Length of pot = 50mm
Diameter of pot = 5mm
FOR THE STILL
Port of thickness = 500mm
Length of pot = 300mm
Diameter of pot = 100mm
FOR THE CONDESER
Condenser thickness = 2mm
Diameter of the connecting = 20mm
Pipe =
Length of pot = 200mm
Diameter of pot = 2mm
Generally, the material used in the construction (open steam distillation column) was mild steel sheet and galvanized sheet.

 

TABLE OF CONTENT

Title page
Letter of transmittal
Dedication
Acknowledgement
Abstract
Table of contents

CHAPTER ONE
1.0 INTRODUCTION

CHAPTER TWO
2.0 literature review
2.1 Distillation processes
2.1.1 Binary distillation
2.1.2 Multi component distillation
2.2 Distillation unit
2.2.1 The batch distillation unit
2.2.2 Simple batch distillation unit
2.2.3 Batch distillation unit with pacification
2.2.4 Continuous distillation unit

CHAPTER THREE
3.1 Properties and selection of material for construction
3.2 Effect of temperature on the mechanical properties
3.1.2 Corrosion and erfosion resistance
3.1.3 Economic consideration (cost)
3.1.4 Contamination
3.1.5 Selection of materials

CHAPTER FOUR
4.1 Fabrication procedure
4.2 Marking out
4.2.1 The column
4.2.2 The condenser
4.2.3 The boiler
4.2.4 The stand
4.2.5 The connection pipes
4.3 Diagrams

CHAPTER FIVE
DISCUSSION

CHAPTER SIX
Conclusion/recommendations
References
Appendices/costing
Tables

CHAPTER ONE

INTRODUCTION
Distillation is a separating technique in which two liquids are separated at essentially the same temperature and pressure. It is also the term used to describe the operation where the vaporization of a liquid mixture yields a vapor phase containing more than one constituents and it is desired to recover one or more of this constituents in a nearly pure state.
It would probably be beneficial to define the terms that describe the process and related properties. Let us begin by describing the process by which a substance transformed from the condensed phase to the gas phase. For liquid, this process is called VAPORIZATION and for a solid it is called SUBMIATIN, both processes requires heat. All substances regardless whether they are liquids or solids are characterized by a vapor pressure. The vapor pressure of a pure substance is the pressure exerted by the substance against the external pressure which is usually atmospheric pressure. Vapor pressure is a measure of the tendency to escape. When the vapor pressure of a liquid substance reaches the external pressure the substance is observed to Boil. If the external pressure is atmospheric pressure, the temperature at which a pure substance boils is called the NORMAL BOILING POINT. Solid substances are not characterized by a similar phenomena called BOILING. They simply vaporize directly into the atmosphere.
Generally speaking, distillation, stripping, absorption, humidification are industrial stage wise operations which involves the contact of two phases in various apparatus. Completion of separation depends upon certain properties of components involved and the arrangement of the distillation process.
The properties involved are:
– Mode of temperature and process control
– The relative volatility between the liquid and vapor phases
– The production capacity of the distiller
– The type of distillation involved
However, the importance of distillation in commercial process is the purification of a large variety of material and petroleum industries. It is applied in the production of hot drinks in chemical industries. Also, applied in oil companies for the separation of petroleum into its various components e.g kerosene, diesel, gasoline, petrol, fuel, oil, lubricating oil, paraffin wax, aliphatic etc. Lastly, it is equally applied in pharmaceutical industries for the production of ethylated spirits and many other medical strubs.

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Project Structure

The introduction of Construction Of An Open Steam Distillation Column should start with the relevant background information of the study, clearly define the specific problem that it addresses, outline the main object, discuss the scope and any limitation that may affect the outcome of your findings

Literature Review of Construction Of An Open Steam Distillation Column should start with an overview of existing research, theoretical framework and identify any gaps in the existing literature and explain how it will address the gaps

Methodology of Construction Of An Open Steam Distillation Column should describe the overall design of your project, detail the methods and tools used to collect data explain the techniques used to analyse the collected data and discuss any ethical issues related to your project

Results should include presentation of findings and interpretation of results

The discussion section of Construction Of An Open Steam Distillation Column should Interpret the implications of your findings, address any limitations of your study and discuss the broader implications of your findings

The conclusion of Construction Of An Open Steam Distillation Column should include summarize the main results and conclusions of your project, provide recommendations based on your findings and offer any concluding remarks on the project.

References should List all the sources cited in Construction Of An Open Steam Distillation Column project by following the required citation style (e.g., APA, MLA, Chicago).

The appendices section should Include any additional materials that support your project (Construction Of An Open Steam Distillation Column) but are too detailed for the main chapters such as raw data, detailed calculations etc.